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ECD-4-nano

ECD-4-nano 型號:ECD-4-nano

Advanced Electrochemical Dilatometer for the measurement of electrode expansion with nanometer resolution.

  • Capacitive displacement sensor (range 250 μm, resolution better than 5 nm)
  • Additional gas pressure (0 to 3 bar) and temperature sensor (-20 to 80° C)
  • Cableless connection via PAT socket, with electronic cell tag (PAT-Button)
  • PRODUCT DETAILS
  • Advanced test cell for the measurement of the electrode expansion in the nanometer range.
    The ECD-4-nano takes dilatometry measurements to the next level
    The ECD-4-nano is a high-resolution electrochemical dilatometer. The most powerful version offers a capacitive parallel plate sensor system with a resolution of better than 5 nanometers. This makes the ECD-4-nano the perfect instrument for detecting thickness changes of the individual electrode or the full cell stack during the electrochemical cycle.
    The ECD-4-nano‘s completely redesigned test cell features a corrosion-resistant cell bottom and a new One-Seal concept that significantly improves tightness over previous ECD-3 models. This enables stable long-term operation as well as the use of a wide range of electrolytes.
    To further improve workflow and handling, we have now integrated the ECD-4-nano into the PAT system. The dilatometer can be inserted directly into a PAT-Tester-x or a docking station such as the PAT-Clamp-1. This allows a space-saving and fast setup of the instrument. Needless to say, the integrated PAT-Button also ensures automatic recognition of the test cell in our EL-Software measurement software.
    Sample Test Results


    Sample Setup


    Sample Setup

    Working principle of the ECD-4-nano (3-electrode setup)
    he working electrode (WE) and the counter electrode (CE) are separated by a stiff glass frit soaked with electrolyte. The upper WE is sealed by means of a flexible metal membrane, through which any charge-induced thickness change is transmitted towards the sensor/load unit attached on top. The fixation of the glass frit ensures that only the thickness change of the working electrode is being detected without interference from the CE.

  • Length 64 mm
    Width 67 mm
    Height 149 mm
    Weight 2 kg  
    Sample diameter 10 mm
    Glass T-Frit (Separator) 12.5/10 x 3.5 mm
    Separator diameter (full cell mode) max. 10 mm
    Working (upper) electrode diameter max. 10 mm
    Counter (lower) electrode diameter max. 12 mm
    Gas pressure sensor: 0 to 3 bar abs.
    Chemical compatibility Aprotic organic electrolytes
    Cell electrolyte volume approx. 0.2 ml
    Operational temperature range (cell and sensor) -20 to 80° C
    Operational temperature range (conditioning electronics and data logger) 0 to 40 °C
    Load on test specimen approx. 1 Newton
     
    Product variants ECD-4-nano ECD-4
     
    Displacement sensor type: Capacitive LVDT
    Displacement range: 250 μm 500 μm
    Displacement resolution: ≤ 5 nm ≤ 50 nm

     

    Compatible PAT docking stations and potentiostats